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In page Geneva Protocol:

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In the Hague Conventions of 1899 and 1907, the use of dangerous chemical agents was outlawed. In spite of this, the First World War saw large-scale chemical warfare. France used tear gas in 1914, but the first large-scale successful deployment of chemical weapons was by the German Empire in Ypres, Belgium in 1915, when chlorine gas was released as part of a German attack at the Battle of Gravenstafel. Following this, a chemical arms race began, with the United Kingdom, Russia, Austria-Hungary, the United States, and Italy joining France and Germany in the use of chemical weapons.[citation needed]